A single-step pesticide extraction and clean-up multi-residue analytical method by selective pressurized liquid extraction followed by on-line solid phase extraction and ultra-high-performance liquid chromatography-tandem mass spectrometry for complex matrices
详细信息 查看全文
- 作者：Elsa Teresa Rodriguesa ; etrodrig@zoo.uc.pt" class="auth_mail" title="E-mail the corresponding author ; Miguel  ; ngelo Pardala ; mpardal@zoo.uc.pt" class="auth_mail" title="E-mail the corresponding author ; Noelia Salgueiro-Gonzá ; lezb ; n.salgueiro@udc.es" class="auth_mail" title="E-mail the corresponding author ; Soledad Muniategui-Lorenzob ; smuniat@udc.es" class="auth_mail" title="E-mail the corresponding author ; Maria Fá ; tima Alpenduradac ; mfalpendurada@iaren.pt" class="auth_mail" title="E-mail the corresponding author
- 关键词：Pesticides ; Environmental samples ; Marine complex matrices ; Selective pressurized liquid extraction ; On-line SPE-UPLC-ESI&ndash ; MS/MS ; Green chemistry
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：24 June 2016
- 年：2016
- 卷：1452
- 期：Complete
- 页码：10-17
- 全文大小：828 K
文摘
- •
Potential hazards of pesticides should be determined to support environmental risk.
- •
Research establishing pesticide residue levels in complex matrices are missing.
- •
Analytical challenges arise to successfully determine these levels in complex matrices.
- •
A multi-residue analytical method for complex matrices was developed and validated.
- •
Developed methods were successfully applied to real environmental marine samples.