Effect of curing light emission spectrum on the nanohardness and elastic modulus of two bulk-fill resin composites

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• 作者：Yaser Issa^a ; David C. Watts^b ; Daniel Boyd^c ; Richard B. Price^d ; ^{rbprice@dal.ca" class="auth_mail" title="E-mail the corresponding author}
• 关键词：Resin based composite ; Bulk fill ; Light curing unit ; Light emitting diode ; Photo polymerization ; Nano-indentation ; Nanohardness ; Elastic modulus ; Emission spectrum
• 刊名：Dental Materials
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：32
• 期：4
• 页码：535-550
• 全文大小：3501 K

文摘

To determine the nanohardness and elastic moduli of two bulk-fill resin based composites (RBCs) at increasing depths from the surface and increasing distances laterally from the center after light curing.

Methods

Two bulk-fill dental RBCs: Tetric EvoCeram Bulk Fill (TECBF) and Filtek Bulk Fill Flowable (FBFF) were light cured in a metal mold with a 6 mm diameter and a 10 mm long semi-circular notch. The RBCs were photo-polymerized for 10 s using a light emitting diode (LED) Bluephase Style curing light, with the original light probe that lacked the homogenizer. This light has two blue light and one violet light LED emitters. By changing the probe orientation over the mold, the light output from only two LEDs reached the RBC. Measurements were made using: (i) the light from one violet and one blue LED, and (ii) the light from the two blue LEDs. Five specimens of each RBC were made using each LED orientation (total 20 specimens). Specimens were then stored in the dark at 37 °C for 24 h. Fifty indents were made using an Agilent G200 nanoindentor down to 4 mm from the surface and 2.5 mm right and left of the centerline. The results were analyzed (alpha = 0.05) using multiple paired-sample t-tests, ANOVA, Bonferroni post-hoc tests, and Pearson correlations.

Results

The elastic modulus and nanohardness varied according to the depth and the distance from the centerline. For TECBF, no significant difference was found between the spatial variations in the elastic modulus or hardness values when violet-blue or blue-blue LEDs were used. For FBFF, the elastic modulus and nanohardness on the side exposed to the violet emitter were significantly less than the side exposed to the blue emitter. A strong correlation between nanohardness and elastic modulus was found in all groups (r² = 0.9512–0.9712).

Significance

Resin polymerization was not uniform throughout the RBC. The nanohardness and elastic modulus across two RBC materials were found to decline differently according to the orientation of the violet and blue light LED emitters within the curing light.