Chiral separation of new designer drugs (Cathinones) on chiral ion-exchange type stationary phases
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- 作者：Denise Wolraba ; b ; Peter Frü ; haufb ; Alena Moulisová ; a ; Martin Kuchařc ; Christopher Gernerb ; Wolfgang Lindnerb ; Michal Kohouta ; michal.kohout@vscht.cz" class="auth_mail" title="E-mail the corresponding author
- 关键词：AcOH ; acetic acid ; ACN ; acetonitrile ; c-SCX ; chiral strong cation exchanger ; DEA ; diethyl amine ; FA ; formic acid ; MeOH ; methanol ; SA ; selectand (analyte) ; SO ; selector ; TEA ; triethyl amine ; TFA ; trifluoroacetic acid ; ZWIX ; zwitterion ion exchange-type stationary phase
- 刊名：Journal of Pharmaceutical and Biomedical Analysis
- 出版年：2016
- 出版时间：20 February 2016
- 年：2016
- 卷：120
- 期：Complete
- 页码：306-315
- 全文大小：1422 K
文摘
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Successful enantioseparation of new designer drugs (Cathinones) was achieved.
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MS-compatible mobile phases and ion-exchange type CSPs were employed.
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Influence of mobile phases and selector structures on enantioseparation was assessed.
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Achiral separation of cathinones with a new ion-exchange type CSP is presented.