Ti₃SiC₂ powder synthesis

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• 作者：Sun ; ZhengMing ; Yang ; Songlan ; Hashimoto ; Hitoshi
• 关键词：A. Powder ; Titanium silicon carbide ; Synthesis
• 刊名：Ceramics International
• 出版年：2004
• 出版时间：2004
• 年：2004
• 卷：30
• 期：7
• 页码：1873-1877
• 全文大小：236 K

文摘

In this article, we report the successful synthesis of single phase Ti₃SiC₂ powder through a simple process by heat treating powder mixtures of Ti, Si, and TiC. By adjusting the composition of the starting powders and the condition of heat treatment, resultant powder with Ti₃SiC₂ content over 99 % was obtained. The intermediate phase of Ti₅Si₃ was found to form which subsequently assisted the formation of the Ti₃SiC₂ phase.