Pre-column dilution large volume injection ultra-high performance liquid chromatography-tandem mass spectrometry for the analysis of multi-class pesticides in cabbages
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- 作者：Qisheng Zhongb ; Lingling Shenb ; Jiaqi Liub ; Dianbao Yub ; Siming Lib ; Jinting Yaob ; Song Zhanb ; Taohong Huangb ; Yuki Hashib ; Shin-ichi Kawanob ; Zhaofeng Liuc ; Ting Zhoua ; d ; tingzhou@scut.edu.cn" class="auth_mail" title="E-mail the corresponding author
- 关键词：Pre-column dilution large volume injection (PD-LVI) ; Ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC&ndash ; MS/MS) ; Column-head stacking ; Pesticides
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：15 April 2016
- 年：2016
- 卷：1442
- 期：Complete
- 页码：53-61
- 全文大小：2537 K
文摘
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A novel sample injection technique PD-LVI for UHPLC–MS/MS was developed.
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The features and mechanism of PD-LVI were systematically investigated.
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The feasibility was demonstrated by analyzing 24 pesticides residues in cabbages.
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PD-LVI could be extended to other LC system without extra complicated accessories.