Determination of polar pesticides in olive oil and olives by hydrophilic interaction liquid chromatography coupled to tandem mass spectrometry and high resolution mass spectrometry
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- 作者：Rocí ; o Nortes-Mé ; ndeza ; José ; Robles-Molinaa ; Rafael Ló ; pez-Blancoa ; Andrea Vassa ; b ; Antonio Molina-Dí ; aza ; c ; Juan F. Garcia-Reyesa ; jfgreyes@ujaen.es" class="auth_mail" title="E-mail the corresponding author
- 关键词：Liquid chromatography/mass spectrometry (LC&ndash ; MS) ; Polar pesticides ; HILIC ; Olive oil ; Olives
- 刊名：Talanta
- 出版年：2016
- 出版时间：1 September 2016
- 年：2016
- 卷：158
- 期：Complete
- 页码：222-228
- 全文大小：620 K
文摘
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Analysis of 7 polar pesticides by HILIC-TOFMS and HILIC-QQQ-MS.
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QuPPe was employed for the extraction of target analytes in olive and olive oil.
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Matrix effects were higher in olive than olive oil methodology.
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The use of tandem mass spectrometry allowed LOQs bellow MRLs for both olive and olive oil.