TiO2 promotes melon to form at 400 °C, whereas it forms at 500 °C for only melamine.
The highest photocatalytic activity was achieved when calcination was performed at 400 °C.
Coordinated NTiN bonds were formed in MA/TiO2 (400) and disappeared at high temperature.
The surface area decreased and the pore size increased with increasing of temperature.
Only MA/TiO2 (400) has a narrower band gap than pure g-C3N4.