An efficient procedure for preparing main acylated pentasaccharides from Polygalae Radix using integrated extraction-adsorption method followed by semi-preparative high performance liquid chromatography
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- 作者：Qiyuan Shi shiqiyuan@zju.edu.cn" class="auth_mail" title="E-mail the corresponding author ; Shu Geng ; Jiale Chen ; Qinfen Zhou ; Ye Jin ; Houliang Lei ; Lianjun Luan ; Xuesong Liu ; Yongjiang Wu ; yjwu@zju.edu.cn" class="auth_mail" title="E-mail the corresponding author
- 关键词：Acylated pentasaccharides ; Polygalae Radix ; Integrated extraction&ndash ; adsorption method ; Semi-preparative high performance liquid chromatography
- 刊名：Separation and Purification Technology
- 出版年：2015
- 出版时间：16 October 2015
- 年：2015
- 卷：153
- 期：Complete
- 页码：84-90
- 全文大小：701 K
文摘
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An efficient method for the extraction of acylated pentasaccharides was proposed.
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The extraction yields of acylated pentasaccharides were improved by more than 38.9%.
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Three main acylated pentasaccharides were prepared by semi-preparative HPLC.