Characterization and determination of isomers in plants using trace matrix solid phase dispersion via ultrahigh performance liquid chromatography coupled with an ultraviolet detector and quadrupole time-of-flight tandem mass spectrometry
详细信息 查看全文
- 作者：Jing-Jing Xu ; Jun Cao ; caojun91@163.com" class="auth_mail" title="E-mail the corresponding author ; Li-Qing Peng ; Wan Cao ; Qiong-Yao Zhu ; Qian-Yun Zhang
- 关键词：β-Cyclodextrin ; Honeysuckle ; Isomer ; Quadrupole time-of-flight tandem mass spectrometry ; Trace matrix solid phase dispersion ; Ultrahigh performance liquid chromatography
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：4 March 2016
- 年：2016
- 卷：1436
- 期：Complete
- 页码：64-72
- 全文大小：1944 K
文摘
- •
A novel application of trace MSPD using β-CD as sorbent is presented.
- •
The proposed method involves the use of UHPLC-UV, Q-TOF/MS and NMR.
- •
The innovative method was efficient and economic for isomers extraction.
- •
The method was applied to a determination of honeysuckle samples.