Cyclodextrin-based ultrasonic-assisted microwave extraction and HPLC-PDA-ESI-ITMSn separation and identification of hydrophilic and hydrophobic components of Polygonum cuspidatum: A green, rapid and effective process
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- 作者：Fangyuan Gaoa ; b ; 1 ; gaofangyuan@outlook.com" class="auth_mail" title="E-mail the corresponding author ; Tingting Zhoua ; 1 ; tingting_zoo@163.com" class="auth_mail" title="E-mail the corresponding author ; Yongsheng Huc ; 1 ; yshu@outlook.com" class="auth_mail" title="E-mail the corresponding author ; Liai Lana ; Yvan Vander Heydend ; yvanvdh@vub.ac.be" class="auth_mail" title="E-mail the corresponding author ; Jacques Crommene ; Guocai Lub ; newdrug@smmu.edu.cn" class="auth_mail" title="E-mail the corresponding author ; Guorong Fana ; guorfan@outlook.com" class="auth_mail" title="E-mail the corresponding author
- 关键词：Polygonum cuspidatum ; Cyclodextrins ; Ultrasound assisted microwave extraction ; HPLC-PDA-ESI-ITMSn ; Fingerprint analysis
- 刊名：Industrial Crops & Products
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：80
- 期：Complete
- 页码：59-69
- 全文大小：2464 K
文摘
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UAME was assessed as most efficient extraction method, compared to HRE, UE and ME.
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Cyclodextrin plays specific roles in the extraction of components from P. cuspidatum.
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An UAME with HP-β-CD as extractant maximized the extraction yields.
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Nineteen compounds were simultaneously identified by HPLC-PDA-ESI-ITMSn.
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Two compounds are firstly reported in P. cuspidatum.