A systematic approach to the synthesis of LDH nanoparticles by response surface methodology

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• 作者：Cecilia Vasti^a ; Valeria Pfaffen^a ; Ernesto Ambroggio^b ; Mauricio R. Galiano^b ; Ricardo Rojas^a ; ^{rrojas@fcq.unc.edu.ar} ; Carla E. Giacomelli^a
• 关键词：Factorial experimental design ; Fluorophore-labeled nanoparticles ; Coprecipitation ; Intercalation compounds ; Confocal microscopy
• 刊名：Applied Clay Science
• 出版年：2017
• 出版时间：1 March 2017
• 年：2017
• 卷：137
• 期：Complete
• 页码：151-159
• 全文大小：1513 K
• 卷排序：137

文摘

A new tool for customization of layered double hydroxide nanoparticles (LDH-NPs) is described. The composition of the synthesis solutions determine LDH-NPs aggregation. Hydrothermal treatment duration is a key parameter to determine particle size. Fluorescein intercalation in LDH-NPs affected by OH– anions competition. Customized LDH-NPs for biological studies with GUVs and cell lines were synthesized.