Application of response surface methodology for air assisted-dispersive liquid- liquid microextraction of deoxynivalenol in rice samples prior to HPLC-DAD analysis and comparison with solid phase extraction cleanup

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• 作者：Mashaallah Rahmani ; ^{rahmani341@hamoon.usb.ac.ir} ; Elham Ghasemi ; Mojtaba Sasani
• 关键词：Deoxynivalenol ; Air assisted-dispersive liquid-liquid microextraction ; Response surface methodology ; Solid phase extraction cleanup ; HPLC-DAD ; Rice
• 刊名：Talanta
• 出版年：2017
• 出版时间：1 April 2017
• 年：2017
• 卷：165
• 期：Complete
• 页码：27-32
• 全文大小：631 K
• 卷排序：165

文摘

A new air assisted-dispersive liquid-liquid microextraction (AA-DLLME) was applied for determination of deoxynivalenol (DON). In the optimization step, response surface methodology was utilized as a design of experiment method. The method was applied for determination of DON in rice samples. AA-DLLME was compared with SPE cleanup.