Crystallization behavior of iron-based amorphous nanoparticles prepared sonochemically

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• 作者：Naoya Enomoto ; ^{enomoto@cstf.kyushu-u.ac.jp} ; Shingo Hirata ; Miki Inada ; Katsuro Hayashi
• 关键词：Sonochemical synthesis ; Iron carbonyl ; Rapid quenching
• 刊名：Ultrasonics Sonochemistry
• 出版年：2017
• 出版时间：March 2017
• 年：2017
• 卷：35
• 期：part_PB
• 页码：563-568
• 全文大小：2199 K
• 卷排序：35

文摘

Sonoprocess of Fe(CO)5 under fair “oxygen-free” atmosphere was examined. A simple but effective characterization using a normal DTA-TG apparatus is proposed. The amorphous product was found to contain ∼14% volatile component on heating.