Multi-residue method for determination of 58 pesticides, pharmaceuticals and personal care products in water using solvent demulsification dispersive liquid-liquid microextraction combined with liquid chromatography-tandem mass spectrometry
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- 作者：Sergiane Souza Caldas ; Caroline Rombaldi ; Jean Lucas de Oliveira Arias ; Liziane Cardoso Marube ; Ednei Gilberto Primel ; eprimelfurg@gmail.com" class="auth_mail" title="E-mail the corresponding author
- 关键词：Dispersive liquid&ndash ; liquid microextraction ; Pharmaceuticals ; Personal care products ; Pesticides ; Liquid chromatography ; Mass spectrometry ; Water samples
- 刊名：Talanta
- 出版年：2016
- 出版时间：1 January 2016
- 年：2016
- 卷：146
- 期：Complete
- 页码：676-688
- 全文大小：1318 K
文摘
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SD-DLLME was employed for the extraction of 58 pesticides and PPCPs from water.
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Solvent demulsification, instead of centrifugation, was used to break up the emulsion.
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Water was used as demulsification solvent instead an organic solvent.
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The method was successfully applied in real water samples.
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The developed method was efficient, fast, easy and environmentally friendly.