Co–Ni–Mo–P/γ-Al2O3 catalysts were synthesized via electroless deposition.
The Co–Ni–Mo–P/γ-Al2O3 catalysts show high catalytic performance.
The Co–Ni–Mo–P/γ-Al2O3 catalysts can be easy separated from the NaBH4 solution.
The catalysts exhibit favorable cycling capability and low activation energy.