Large multiresidue analysis of pesticides in edible vegetable oils by using efficient solid-phase extraction sorbents based on quick, easy, cheap, effective, rugged and safe methodology followed by gas chromatography-tandem mass spectrometry
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- 作者：P. Parrilla Vá ; zquez ; E. Hakme ; S. Uclé ; s ; V. Cutillas ; M. Martí ; nez Galera ; A.R. Mughari ; A.R. Ferná ; ndez-Alba ; amadeo@ual.es" class="auth_mail" title="E-mail the corresponding author
- 关键词：GC&ndash ; MS/MS ; Edible vegetable oils ; Multiresidue pesticide analysis ; Procedural Standard Calibration ; EMR-Lipid
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：9 September 2016
- 年：2016
- 卷：1463
- 期：Complete
- 页码：20-31
- 全文大小：1676 K
文摘
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Multiresidue method for edible vegetable oils using GC–MS/MS.
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Evaluation of different sorbents for the clean-up step using QuEChERS methodology.
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Comparison of the novel EMR-Lipid sorbent with Z-Sep and PSA.
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Procedural Standard Calibration to correct recovery losses.
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Several pesticides are detected in most of the olive oil samples.