Thermal analysis of bis(tetraethylammonium) tetrachloroferrate(II)
详细信息 查看全文
- 作者：Emilia Styczeń ; Agnieszka Pattek-Janczyk ; Maria Gazda ; Wojciech K. Jó ; ź ; wiak ; Dariusz Wyrzykowski ; Zygmunt Warnke
- 关键词：Tetrahalogenoferrates(II) ; Thermal decomposition ; Mö ; ssbauer spectroscopy
- 刊名：Thermochimica Acta
- 出版年：2008
- 出版时间：15 December 2008
- 年：2008
- 卷：480
- 期：1-2
- 页码：30-34
- 全文大小：211 K
文摘
Thermal decomposition of bis(tetraethylammonium) tetrachloroferrate(II) has been studied using the TG-FTIR, TG–MS and DTA techniques. The measurements were carried out in an inert atmosphere over the temperature range of 293–1073 K. The solid products of the thermal decomposition were identified by the FT-FIR, Mössbauer spectroscopy as well as the X-ray powder diffractometry. The influence of the oxidation state and the nature of a metal on thermal transformation profiles of analogous complexes have been discussed.