Controlled Flow Precipitation as a Valuable Tool for Synthesis

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• 作者：Paolo Filipponi ; Antimo Gioiello ; Ian R. Baxendale
• 刊名：Organic Process Research & Development
• 出版年：2016
• 出版时间：February 19, 2016
• 年：2016
• 卷：20
• 期：2
• 页码：371-375
• 全文大小：328K
• ISSN：1520-586X

文摘

In most standard flow process, the formation of solids represents a major problem often leading to obstruction of the flow device and reactor shutdown. However, many reactions produce solid products, and therefore finding ways to process these materials is an important area of research. In this article we demonstrate how a dynamically agitated flow reactor can be a powerful tool to facilitate workup and processing of biphasic solid–liquid flow streams at scale.