A General NMR Approach for the Structural Determination of Alkaloids: Application to 3--Hydroxylupanine
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- 作者：André ; Touché ; Didier Courtois ; Jean-Paul Frè ; che ; Norbert Bromet ; Florence Djedaï ; ni-Pilard ; Bruno Perly ; Gé ; rald Guillaumet ; and Patrick Rollin
- 刊名：Journal of Agricultural and Food Chemistry
- 出版年：1997
- 出版时间：June 1997
- 年：1997
- 卷：45
- 期：6
- 页码：2148 - 2152
- 全文大小：246K
- 年卷期：v.45,no.6(June 1997)
- ISSN：1520-5118
文摘
The structure of 3-
-hydroxylupanine, a major alkaloid isolated fromthe seeds of Lupinus mutabilisS., was unequivocally established through dedicated 1H and13C NMR experiments, thus revealinga novel general strategy for error-free structural assignment of lupinealkaloids.Keywords: Lupinus mutabilis; Leguminosae; structural analysis; quinolizidinealkaloids; NMR
-hydroxylupanine, a major alkaloid isolated fromthe seeds of Lupinus mutabilisS., was unequivocally established through dedicated 1H and13C NMR experiments, thus revealinga novel general strategy for error-free structural assignment of lupinealkaloids.Keywords: Lupinus mutabilis; Leguminosae; structural analysis; quinolizidinealkaloids; NMR