Synthesis of Ionic Liquids Equipped with 2-Methoxyethoxymethyl/Methoxymethyl Groups Using a Simple Microreactor System
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- 作者：Toshiki Nokami ; Kuninobu Matsumoto ; Taka-aki Itoh ; Yukinobu Fukaya ; Toshiyuki Itoh
- 刊名：Organic Process Research & Development
- 出版年：2014
- 出版时间：November 21, 2014
- 年：2014
- 卷：18
- 期：11
- 页码：1367-1371
- 全文大小：379K
- ISSN：1520-586X
文摘
A simple microreactor system has been utilized for the continuous flow synthesis of novel ionic liquids having a (2-methoxyethoxy)methyl or methoxymethyl substituent. Conversion rates of N-bases and tributylphosphine in the microreactor system are faster than those in the batch system because of less diffusion distance in the tube reactor. This method allows us to prepare ionic liquids in efficient yields with high purity.