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A variety of 1,3,5-tricarbonyl derivatives were prepared by reaction of 1,3-bis(silyl enol et
hers) wit
hacid c
hlorides under mild conditions. T
his includes reactions of bot
h aromatic and alip
hatic acid c
hloridesand bis(acid c
hlorides). T
he yields vary depending on t
he type of acid c
hloride employed.