Simple and Rapid Synthesis of Fe(PO3)3 by Microwave Sintering

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• 作者：Weijia Zhou ; Wen He ; Xudong Zhang ; Jianan Liu ; Yi Du ; Shunpu Yan ; Xiuyin Tian ; Xianan Sun ; Xiuxiu Han ; Yuanzheng Yue
• 刊名：Journal of Chemical & Engineering Data
• 出版年：2009
• 出版时间：July 9, 2009
• 年：2009
• 卷：54
• 期：7
• 页码：2073-2076
• 全文大小：129K
• 年卷期：v.54,no.7(July 9, 2009)
• ISSN：1520-5134

文摘

Fe(PO₃)₃ with different morphologies has been synthesized using H₃PO₄ and Fe₂O₃ as starting compounds by microwave sintering. The structure and morphologies of resultant samples were characterized by X-ray diffractometry, thermogravimetry/differential scanning calorimetry, Fourier transform infrared spectroscopy, and transmission electron microscopy. The Fe(PO₃)₃ crystals obtained from microwave sintering have high thermal stability and good micromorphology. The crystal transformation of Fe(PO₃)₃ and the synthesis mechanism are simply discussed.