Effect of Gold Modification with 3-Mercaptopropionic Acid, Cysteamine and Gold Nanoparticles on Monoethanolamine Electrooxidation

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• 作者：Maria Bełtowska-Brzezinska ; Alicja Zmaczyńska ; Teresa Łuczak
• 关键词：Gold electrode ; Gold nanoparticles ; Self ; assembled layer ; Electrooxidation
• 刊名：Electrocatalysis
• 出版年：2016
• 出版时间：January 2016
• 年：2016
• 卷：7
• 期：1
• 页码：79-86
• 全文大小：868 KB
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• 作者单位：Maria Bełtowska-Brzezinska (1)
  Alicja Zmaczyńska (1)
  Teresa Łuczak (1)
  
  1. Adam Mickiewicz University in Poznań, Department of Chemistry, Umultowska 89 b, PL-61-614, Poznań, Poland
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Electrochemistry
  Physical Chemistry
  Energy Technology
  
• 出版者：Springer New York
• ISSN：1868-5994

文摘

In this work, a gold electrode modified with self-assembled layers (SAMs) composed of 3-mercaptopropionic acid, cysteamine and gold nanoparticles was prepared. The electrode with SAMs endowed with gold nanoparticles gave the high catalytic effect for monoethanolamine (MEA) electrooxidation in solution at pH 7. For this novel sensor, a linear relationship between the current response of MEA at the potential of peak maximum (j _p) and the concentration of this compound in solution (c _MEA) was found, over the range 0.1 μM to 0.8 M with the detection sensitivity equal to about 5 A cm−2 mol−1 dm3 (at v = 0.1 V s−1) and the detection limit of 0.046 μM. Keywords Gold electrode Gold nanoparticles Self-assembled layer Electrooxidation