Synthesis and Characterization of Superparamagnetic NiBaO2 Nano-Oxide Using Novel Precursor Complex [Ba(H2O)8][Ni(dipic)2]
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- 作者：Hamideh Saravani ; Milad Takhsha Ghahfarokhi…
- 关键词：Nano ; oxide ; Thermal decomposition ; XRD ; VSM
- 刊名：Journal of Inorganic and Organometallic Polymers and Materials
- 出版年：2016
- 出版时间：May 2016
- 年：2016
- 卷：26
- 期：3
- 页码：660-666
- 全文大小：936 KB
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Milad Takhsha Ghahfarokhi (1)
Masoud Rafigh Esmaeilzaei (1)
1. Inorganic Chemistry Laboratory, Department of Chemistry, University of Sistan and Baluchestan, Zahedan, 98135-674, Iran - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Inorganic Chemistry
Organic Chemistry
Polymer Sciences - 出版者：Springer New York
- ISSN：1574-1451
文摘
In this paper, for the first time, synthesis of [Ba(H2O)8][Ni(dipic)2] complex and preparation of NiBaO2 nano-oxide are reported through thermal decomposition under surfactant free condition. This novel complex was characterized by Fourier transform infrared spectroscopy (FT-IR), ultra violet–visible spectroscopy, conductivity measurement and elemental analysis. Formation of novel nanoparticles was supported by FT-IR and energy-dispersive X-ray spectroscopy and the orthorhombic structure of nanocrystals was confirmed by powder X-ray diffraction analysis. In addition, size distribution as well as uniform morphology of prepared nano-oxide were recorded by dynamic light scattering analysis and field-emission scanning electron microscopy, respectively. Magnetic features measured by vibrating sample magnetometer, illustrate superparamagnetic behavior of the oxide.