Structure of friction-transferred highly oriented poly(3-hexylthiophene) thin films

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• 作者：Li-guo Chai ; Hai-xin Zhou ; Xiao-li Sun ; Hui-hui Li…
• 关键词：Poly(3 ; hexylthiophene) ; Friction ; transfer ; Thin film ; Orientation
• 刊名：Chinese Journal of Polymer Science
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：34
• 期：4
• 页码：513-522
• 全文大小：1,823 KB
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• 作者单位：Li-guo Chai (1)
  Hai-xin Zhou (1)
  Xiao-li Sun (1)
  Hui-hui Li (1)
  Shou-ke Yan 闫寿科 (1)
  Xiao-qiu Yang (2)
  
  1. State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, China
  2. Basic Research Service, MOST, Beijing, 100862, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Condensed Matter Physics
  Industrial Chemistry and Chemical Engineering
  Polymer Sciences
  Characterization and Evaluation of Materials
  
• 出版者：Chinese Chemical Society and Institute of Chemistry, CAS, co-published with Springer
• ISSN：1439-6203

文摘

Oriented thin films of P3HT were obtained by a friction-transfer technique. The morphology and structure of the film were studied by means of optical microscopy, atomic force microscopy and transmission electron microscopy. Optical microscopy observation indicates that large size well-ordered P3HT thin films can be produced by a friction-transfer technique. Highly ordered lamellae were observed in P3HT friction-transferred films by electron microscopy. Electron diffraction results confirm the existence of high orientation with the a- and c-axes of P3HT crystals aligned in the film plane while the c-axis parallel to the friction-transfer direction. The atomic force microscopy observation of the as-prepared P3HT thin film shows, however, a featureless top surface morphology, indicating the structure inhomogeneity of the obtained film. To get highly oriented P3HT thin films with homogenous structure, high temperature annealing, solvent vapor annealing and self-seeding recrystallization of the friction-transferred film were performed. It is confirmed that solvent vapor annealing and self-seeding recrystallization methods are efficient in improving the surface morphology and structure of the frictiontransferred P3HT thin film. Highly oriented P3HT films with unique structure can be obtained through friction-transfer with subsequent solvent vapor annealing and self-seeding recrystallization. Keywords Poly(3-hexylthiophene) Friction-transfer Thin film Orientation