Preparation of manganese-based perovskite nanoparticles using a reverse microemulsion method: biomedical applications

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• 作者：MEYSAM SOLEYMANI ; MOHAMMAD EDRISSI
• 刊名：Bulletin of Materials Science
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：39
• 期：2
• 页码：487-490
• 全文大小：696 KB
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Materials Science
  Engineering, general
  
• 出版者：Springer India
• ISSN：0973-7669
• 卷排序：39

文摘

In this study, La_0.7Sr_0.3Mn_0.98Ti_0.02O₃ (LSMTO) nanoparticles with a perovskite structure and an average particle size of 23.5 nm were synthesized using a reverse microemulsion method. In this method, cetyltrimethylammonium bromide (CTAB) was used as a surfactant, 1-butanol as a co-surfactant, n-hexane as a continuous oil phase, and an aqueous solution containing metal cations or precipitating agent as a dispersed aqueous phase. The aqueous nanodroplets of microemulsions were used for the formation of perovskite precursor. The obtained precursor was then calcined at 700∘C for 4 h to convert the precursor to the perovskite phase. In addition, the heating ability of the LSMTO nanoparticles was evaluated under a safe alternating magnetic field used in magnetic hyperthermia therapy. The results showed the fast magneto-temperature response of the prepared sample with sufficient heat loss at the therapeutic temperature range, indicating the LSMTO nanoparticles can be used as a self-regulated heating agent in the magnetic hyperthermia therapy.KeywordsReverse microemulsionhyperthermiamagnetic nanoparticlesheat generation