Spectroscopic studies on tungstoheteropolyanions functionalized by amino acids

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• 作者：M. Mirzaei ; H. Eshtiagh-Hosseini ; M. Arefian…
• 关键词：Polyoxometalates ; Amino acids ; Noncovalant interactions ; van der Waals contacts ; Spectroscopic studies
• 刊名：Journal of the Iranian Chemical Society
• 出版年：2015
• 出版时间：July 2015
• 年：2015
• 卷：12
• 期：7
• 页码：1191-1198
• 全文大小：814 KB
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• 作者单位：M. Mirzaei (1)
  H. Eshtiagh-Hosseini (1)
  M. Arefian (1)
  F. Akbarnia (1)
  F. Miri (1)
  S. Edalatkar-Moghadam (2)
  M. Shamsipur (3)
  
  1. Department of Chemistry, Ferdowsi University of Mashhad, 91775-1436, Mashhad, Iran
  2. Department of Chemistry, Yadegar-e Emam Branch, Islamic Azad University, Tehran, Iran
  3. Department of Chemistry, Razi University, Kermanshah, Iran
  
• 刊物主题：Analytical Chemistry; Inorganic Chemistry; Physical Chemistry; Biochemistry, general; Organic Chemistry;
• 出版者：Springer Berlin Heidelberg
• ISSN：1735-2428

文摘

The 19 new inorganic–organic hybrid compounds based on Keggin, Preyssler and Wells–Dawson types of tungstoheteropolyanions and fairly complete series of essential amino acids were prepared and the structure of these materials investigated on the basis of CHN analysis and multi-spectroscopic investigations (IR, 1HNMR and 13CNMR). Changes in position and shape of asymmetric stretching vibration bands in finger print regions of polyoxometalates (POMs) were identified in all FT-IR spectra. These changes are related to noncovalent interactions between POM surface oxygen atoms and the bio-organic molecules. In reported compounds, 12 natural amino acids out of 20 (i.e., alanine, glycine, glutamine, asparagine, methionine, cysteine, leucine, arginine, threonine, aspartic acid, disodium glutamate) have participated.