Preconcentration and Simultaneous Determination of Heterocyclic Aromatic Amines in Grilled Pork Samples by Ion-Pair-Based Surfactant-Assisted Dispersive Liquid-Liquid Microextraction and High-Performance Liquid Chromatography

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• 作者：Jitlada Vichapong ; Supalax Srijaranai…
• 关键词：Dispersive liquid ; liquid microextraction ; Ion pair extraction ; Heterocyclic aromatic amines ; Grilled pork samples ; HPLC
• 刊名：Food Analytical Methods
• 出版年：2016
• 出版时间：May 2016
• 年：2016
• 卷：9
• 期：5
• 页码：1120-1127
• 全文大小：412 KB
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• 作者单位：Jitlada Vichapong (1)
  Supalax Srijaranai (2)
  Yanawath Santaladchaiyakit (3)
  Wanna Kanchanamayoon (1)
  Rodjana Burakham (2)
  
  1. Creative Chemistry and Innovation Research Unit, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Mahasarakham University, Mahasarakham, 44150, Thailand
  2. Materials Chemistry Research Center, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Khon Kaen University, Khon Kaen, 40002, Thailand
  3. Department of Chemistry, Faculty of Engineering, Rajamangala University of Technology Isan, Khon Kaen Campus, Khon Kaen, 40000, Thailand
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Food Science
  Chemistry
  Microbiology
  Analytical Chemistry
  
• 出版者：Springer New York
• ISSN：1936-976X

文摘

An effective ion-pair-based surfactant-assisted dispersive liquid-liquid microextraction combined with high-performance liquid chromatography (HPLC) has been evaluated for the extraction and preconcentration of four heterocyclic aromatic amines (i.e., 2-amino-3,4-dimethyl-3H-imidazo[4,5-f]quinoline (MeIQ); 2-amino-3,4,8-trimethyl-3H-imidazo[4,5-f]quinoxaline (4,8-DiMeIQx); 2-amino-1-methyl-6-phenylimidazo[4,5-b]pyridine (PhIP); and 1-methyl-9H-pyrido[3,4-B]indole (Harmane)). In the extraction method, sodium dodecyl sulfate (SDS) was used as both ion-pairing and disperser agent and 1-octanol was selected as extraction solvent. The effects of various parameters on the extraction efficiency such as kind and concentration of surfactant, kind and volume of extraction, salt addition, vortex extraction, and centrifugation time were investigated. Under the selected condition, the method provided high enrichment factor in the ranged of 124–145. Good linearity was 0.01–1000 μg kg−1 with the correlation coefficient (R 2) > 0.999. The limit of detection was 0.01 μg kg−1 for all compounds. The matrix match calibration was used for quantitation of the target analytes in grilled pork samples. The proposed method was successfully applied to analysis of heterocyclic aromatic amines in grilled pork samples where good recoveries were obtained in the range of 90 and 106 %.