Spectral and thermal characterization of grown organic single crystal

详细信息    查看全文

• 作者：S. Janarthanan (1)
  R. Sugaraj Samuel (2)
  Y. C. Rajan (3)
  P. R. Umarani (1)
  S. Pandi (1) drspandi@gmail.com
• 关键词：Crystal growth &#8211 ; X ; ray diffraction &#8211 ; Optical material &#8211 ; Thermal studies
• 刊名：Journal of Thermal Analysis and Calorimetry
• 出版年：2012
• 出版时间：July 2012
• 年：2012
• 卷：109
• 期：1
• 页码：69-72
• 全文大小：391.1 KB
• 参考文献：1. Gunter P, Bosshard Ch, Shutter K, Arend H, Chapuis G, Twisg RJ, Dobrowolski D. 2-cyclooctylamino-5-nitropyridine, a new nonlinear optical crystal with orthorhombic symmetry. Appl Phys Lett. 1987;50:486–8.
  2. Tao XT, Yuan DR, Zhang N, Jiang MH, Shao ZS. Novel organic molecular second harmonic generation crystal: 3-methoxy-4-hydroxy-benzaldehyde. Appl Phys Lett. 1992;60:1415–7.
  3. Badan J, Hierle R, Perigaud A, Zyss J. Nonlinear optical properties of organic molecules and polymeric material. In: Williams DJ, editor. American Chemical Symposium Series, vol 233. Washington: American Chemical Society; 1993.
  4. Chemla DS, Zyss J. Nonlinear optical properties of organic molecules and crystals, vol I & II. New York: Academic; 1987.
  5. Nalwa HS, Miyata S. Nonlinear optics of organic molecules and polymers. Boca Raton, FL: CRC Press; 1997.
  6. Bosshard C, Sutter K, Pretre P, Hulliger J, Floersheimer M, Kaatz P, Guenter P. Organic nonlinear optical materials. Amsterdam: Cordon and Breach; 1995.
  7. Sukhorukov AA, Kivshar YS. Nonlinear guided waves and spatial solutions in a periodic layered medium. J Opt Soc Am. 2002;19B:772–8.
  8. Maroulis G. Static hyperpolarizability of the water dimmer and the interaction hyperpolarizability of two water molecules. J Chem Phys. 2000;113:1813–20.
  9. Maroulis G. Electric multipole moment, dipole and quadrupole (hyper) polarizability derivatives for HF (X 1Σ +). J Mol Struct (Theochme). 2003;633:177–97.
  10. Schoonveld WA, Wildeman J, Fichou D, Bobbert PA, Van Wees BJ, Klapwijk TM. Coulomb-blockade transport in single-crystal organic thin-film transistors. Nature. 2000;404:977–80.
  11. Rappoport Z. CRC hand book of tables for organic compound identification. 2nd ed. Boca Raton, FL: CRC Press; 1984.
  12. Shriner RL, Fussion RC, Curtin DY, Morrill TC. The systematic identification of organic compounds. 6th ed. New York: John Wiley & Sons; 1980.
  13. Mojumdar SC, Raki L. Preparation, thermal spectral and microscopic studied of calcium silicate hydrate-poly(acrylic acid) nanocomposite materials. J Therm Anal Calorim. 2006;85:99–105.
  14. Madurambal G, Mariappan M, Majumdar SC. Thermal, UV and FTIR spectral studies of urea–thiourea zinc chloride single crystal. J Therm Anal Calorim. 2010;100:763–8.
  15. Meenakshisundaram SP, Parthiban S, Madhrambal G, Majumdar SC. Effect of chelating agent (1, 10-phenanthroline) on potassium hydrogen phthalate crystal. J Therm Anal Calorim. 2008;94:21–5.
  16. Rajasekaran M, Anbusrinivasan P, Mojumdar SC. Growth, spectral and thermal characterization of 8-hydroxyquinoline. J Therm Anal Calorim. 2010;100:827–30.
  17. Ondrusova D, Jona E, Simon P. Thermal properties of N-ethyl-N phenyldithiocarbamates and their influence on the kinetics of cure. J Therm Anal Calorim. 2002;67:147–52.
  18. Verma RK, Verma L, Ranjan M, Verma BP, Mojumdar SC. Thermal analysis of 2-oxocyclopentanedithiocarboxylato complexes of iron(III), copper(II) and zinc(II) containing pyridine or morpholine as the second ligand. J Therm Anal Calorim. 2008;94:27–31.
  19. Madhurambal G, Ramasamy P, Anbusrinivasan P, Vasudevan G, Kavitha S, Mojumdar SC. Growth and characterization studies of 2-bromo-40-chloro-acetophenone (BCAP) crystals. J Therm Anal Calorim. 2008;94:59–62.
  20. Madhurambal G, Mariappan M, Mojumdar SC. TG–DTA, UV and FTIR spectroscopic studies of urea–thiourea mixed crystal. J Therm Anal Calorim. 2010;100:853–6.
  21. Madhurambal G, Ravindran B, Mariappan M, Mojumdar SC. Thermal, UV and FTIR spectral studies in alkali metal cinnamates. J Therm Anal Calorim. 2010;100:811–5.
  22. Furniss BS, Hannaford AJ, Smith PWG, Tatchell AR. Vogels text book of practical organic chemistry, 5th ed. London: English Language Book Society, Chapman and Hall; 1996.
  23. Kurtz SK, Perry TT. A powder technique for the evaluation of nonlinear optical materials. J Appl Phys. 1968;39:3798–813.
• 作者单位：1. Department of Physics, Presidency College, Chennai, India2. Department of Chemistry, Presidency College, Chennai, India3. Department of Materials Science, National Chiao Tung University, Hsinchu, Taiwan, ROC
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Sciences
  Polymer Sciences
  Physical Chemistry
  Inorganic Chemistry
  Measurement Science and Instrumentation
  
• 出版者：Akad茅miai Kiad贸, co-published with Springer Science+Business Media B.V., Formerly Kluwer Academic
• ISSN：1572-8943

文摘

The growth of semicarbazone of p-hydroxy benzaldehyde (SPHB) single crystal by slow evaporation solution growth technique is reported in this article. The grown crystal was subjected to powder XRD study to identify the crystalline nature. Single crystal XRD study was done to measure unit cell parameters and to confirm the crystal structure. In the presence of various functional groups of SPHB was identified by FTIR spectrum. Its optical behavior was examined by UV–Vis–NIR spectrum and the crystal was found to have transparency in the region between 245 and 1100 nm. Thermal properties of the crystal were investigated using thermogravimetric and differential thermal analysis (TG-DTA), which indicated that the melting of the material occurred before decomposition. The nonlinear optical (NLO) property was tested by Kurtz–Perry powder technique for second harmonic generations.