Structural, morphological and electrical studies of BaCe0.8Y0.2O3-δ synthesized by solution combustion method
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- 作者：S. T. Jadhav ; S. U. Dubal ; A. P. Jamale ; S. P. Patil ; C. H. Bhosale ; V. R. Puri…
- 关键词：Chemical synthesis ; Oxides ; Sintering ; Thermogravimetric analysis ; Crystal structure ; Electrical properties
- 刊名：Ionics
- 出版年：2015
- 出版时间：May 2015
- 年：2015
- 卷：21
- 期：5
- 页码：1295-1300
- 全文大小：1,044 KB
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- 刊物主题：Chemistry
Electrochemistry
Materials Science
Physical Chemistry
Condensed Matter
Renewable Energy Sources
Electrical Power Generation and Transmission - 出版者：Springer Berlin / Heidelberg
- ISSN：1862-0760
文摘
The 20?% yttrium doped barium cerate (BCY20) powder has been synthesized by cost effective solution combustion method. The flame temperature measured by pyrometer was 1055?°C, less than the adiabatic temperature due to various losses. The phase formation and evolution was studied with TG-DTA and XRD. The carbonate free orthorhombic BCY20 phase was obtained upon calcination at 900?°C. The microstructure of the powders and sintered pellet was examined through scanning electron microscopy. The vibrational mode at 355?cm, characteristics of CeO6 octahedra, was detected in Raman while the bands corresponding to M-O vibrations were revealed in FT-IR. The dc conductivities of sintered pellet measured in argon and air atmospheres at 600?°C were 1.53?×-0? and 1.41?×-0??S/cm.