A novel ionic liquid synthesis, electrochemical polymerization, and sensing performance toward bisphenol A

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• 作者：Jia Zhao ; Yanhui Ma ; Xiaodong Hou ; Liqing Li…
• 关键词：Ionic liquid ; Electrochemical polymerization ; Sensor ; Bisphenol A
• 刊名：Journal of Solid State Electrochemistry
• 出版年：2015
• 出版时间：June 2015
• 年：2015
• 卷：19
• 期：6
• 页码：1571-1578
• 全文大小：561 KB
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• 作者单位：Jia Zhao (1)
  Yanhui Ma (2)
  Xiaodong Hou (3)
  Liqing Li (3)
  Peifeng Zheng (3)
  Chunya Li (2)
  
  1. College of Resources & Environment, Hunan Agricultural University, Changsha, 410128, China
  2. Laboratory of Analytical Chemistry of the Satate Ethnic Affairs Commission, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan, 430074, China
  3. Chaozhou Quality and Measurement Supervision and Inspection Institute, Chaozhou, 521011, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Physical Chemistry
  Analytical Chemistry
  Industrial Chemistry and Chemical Engineering
  Characterization and Evaluation Materials
  Condensed Matter
  Electronic and Computer Engineering
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1433-0768

文摘

A novel 1-[3-(tert-butoxycarbonylamino)propyl]-3-[3-(N-pyrrole)propyl]imidazolium tetrafluoroborate ionic liquid was successfully synthesized and was used as functional monomer to electrochemically fabricate a polymer film modified glassy carbon electrode (Poly-IL/GCE). Morphology and the interfacial property of Poly-IL/GCE were examined with scanning electron microscope and electrochemical impedance spectroscopy, respectively. Bisphenol A (BPA) was chosen as a model compound to investigate the sensing performance of Poly-IL/GCE using voltammetry. The oxidation peak currents of BPA at the Poly-IL/GCE exhibit a linear response to its concentration in the range of 1.0?×-0--.0?×-0-?M. The detection limit is calculated to be 4.0?×-0-?M (S/N--). The Poly-IL/GCE was successfully applied to analysis BPA leaching from drinking water bottle. The results are consistent with that of high-performance liquid chromatography.