Synthesis and characterization of pyridine-4-carboxylic acid functionalized Fe3O4 nanoparticles as a magnetic catalyst for synthesis of pyrano[3,2-b]pyranone deriv
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- 作者：Sakineh Asghari ; Majid Mohammadnia
- 关键词：Magnetic properties ; Pyrano[3 ; 2 ; b]pyranone ; Arylaldehydes ; Kojic acid ; Ethyl cyanoacetate ; Nanoparticles
- 刊名：Research on Chemical Intermediates
- 出版年：2016
- 出版时间：March 2016
- 年：2016
- 卷：42
- 期：3
- 页码：1899-1911
- 全文大小：1,498 KB
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35.R. Pielaszek, J. Appl. Crystallogr. 1, 43–50 (2003) - 作者单位：Sakineh Asghari (1) (2)
Majid Mohammadnia (1)
1. Department of Organic Chemistry, Faculty of Chemistry, University of Mazandaran, 47416-95447, Babolsar, Iran
2. Nano and Biotechnology Research Group, University of Mazandaran, Babolsar, Iran - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Catalysis
Physical Chemistry
Inorganic Chemistry - 出版者：Springer Netherlands
- ISSN：1568-5675
文摘
Pyridine-4-carboxylic acid (PYCA) functionalized Fe3O4 nanoparticles as an organic–inorganic hybrid heterogeneous catalyst was fabricated and characterized by FT-IR, XRD, TGA, TEM, SEM, and VSM techniques. The catalytic activity of the magnetic catalyst was probed through one-pot synthesis of pyrano[3,2-b]pyranone derivatives from three component reactions of aromatic aldehydes, kojic acid, and ethyl cyanoacetate under solvent-free conditions. Some advantages of this protocol are its environmentally benign method, simple procedure, high yields, and short reaction time. The catalyst was readily separated using an external magnet and reusable without significant loss of its catalytic efficiency.