Temperature and Frequency Dependence on Electrical Properties of Fe3O4@ Caffeic Acid Nanocomposite
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- 作者：A. Baykal ; H. Erdemi ; Md. Amir
- 关键词：Fe3O4 ; Caffeic acid ; Conductivity ; Dielectric properties ; Spinel compounds
- 刊名：Journal of Inorganic and Organometallic Polymers and Materials
- 出版年：2016
- 出版时间：January 2016
- 年：2016
- 卷：26
- 期：1
- 页码：190-196
- 全文大小：1,518 KB
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H. Erdemi (2)
Md. Amir (1)
1. Department of Chemistry, Fatih University, Büyükçekmece, 34500, Istanbul, Turkey
2. Department of Polymer Engineering, Yalova University, 77100, Yalova, Turkey - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Inorganic Chemistry
Organic Chemistry
Polymer Sciences - 出版者：Springer New York
- ISSN：1574-1451
文摘
This study reports the refflux synthesis and dielectrical characterization of caffeic acid coated magnetite (Fe3O4) nanoparticles. Rietveld refinement confirmed the single phase product formation with the average crystallite size of 11.4 nm by Scherrer Formula. The coating of caffeic acid on the surface Fe3O4 nanoparticles was monitored by Fourier transform infrared spectroscopy, the interaction being via bridging oxygens of the carboxylate and the nanoparticle surface. ac/dc conductivity and dielectric analyses of product revealed semiconductor characteristics varying with temperature. ac conductivity increases regularly with temperature and do not show frequency-dependent behavior particularly at lower frequency regime whereas it exhibits a significant temperature dependent behavior at medium frequencies and at higher temperatures. Keywords Fe3O4 Caffeic acid Conductivity Dielectric properties Spinel compounds