Gold nanoparticles-based colorimetric determination of cationic surfactants in environmental water samples via both electrostatic and hydrophobic interactions

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• 作者：Kamlesh Shrivas ; Swapan Sahu ; Anupam Ghorai ; Ravi Shankar
• 关键词：Colorimetric probe ; Tatrate capping ; TEM ; Aggregation ; Environmental analysis
• 刊名：Microchimica Acta
• 出版年：2016
• 出版时间：February 2016
• 年：2016
• 卷：183
• 期：2
• 页码：827-836
• 全文大小：1,382 KB
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• 作者单位：Kamlesh Shrivas (1)
  Swapan Sahu (1)
  Anupam Ghorai (1)
  Ravi Shankar (2) (3)
  
  1. Department of Chemistry, Guru Ghasidas Vishwavidyalaya, Bilaspur, CG, 495009, India
  2. Nanoscience and Nanoengineering Program, South Dakota School of Mines and Technology, Rapid City, SD, 57701, USA
  3. Fujifilm Imaging Colorants, Inc, 233 Cherry Lane, New Castle, DE, 19720, USA
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Analytical Chemistry
  Inorganic Chemistry
  Physical Chemistry
  Characterization and Evaluation Materials
  Monitoring, Environmental Analysis and Environmental Ecotoxicology
  
• 出版者：Springer Wien
• ISSN：1436-5073

文摘

We report on a simple, rapid and sensitive colorimetric assay for the quantitation of cationic surfactants (CS+) in domestic effluent, municipal waste and surface water samples. The method is based on the aggregation of tartrate-capped gold nanoparticles (AuNPs) through both electrostatic and hydrophobic interactions that occur between CS+ and AuNPs. Aggregation results in a color change from pink to blue which is due to a shift in the localized surface plasmon resonance band. The detergent cetylpyridinium chloride (CPC) was chosen as a model compound for optimization of the method for determination of a CS+. Under optimized experimental conditions (pH 9.0; reaction time 5 min; 25 nM concentration of AuNPs), a linear calibration plot was obtained for quantitative determination of CPC, cetyltrimethylammonium bromide (CTAB), dodecyltrimethyl ammonium bromide (DTAB) in the range of 10–500, 10–200 and 10–300 ngmL−1, respectively and the limit of detection was 3 ngmL−1 for CPC, CTAB and DTAB.