Polyfluorinated substances in abiotic standard reference materials

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• 作者：Jessica L. Reiner (1) (2)
  Andrea C. Blaine (3)
  Christopher P. Higgins (3)
  Carin Huset (4)
  Thomas M. Jenkins (5)
  Christiaan J. A. F. Kwadijk (6)
  Cleston C. Lange (7)
  Derek C. G. Muir (8)
  William K. Reagen (7)
  Courtney Rich (3)
  Jeff M. Small (8)
  Mark J. Strynar (9)
  John W. Washington (5)
  Hoon Yoo (5)
  Jennifer M. Keller (2)
  
  1. Chemical Sciences Division ; National Institute of Standards and Technology ; 100 Bureau Dr. ; Mail Stop 8392 ; Gaithersburg ; MD ; 20899-8392 ; USA
  2. Chemical Sciences Division ; National Institute of Standards and Technology ; 331 Ft. Johnson Road ; Charleston ; SC ; 29412 ; USA
  3. Colorado School of Mines ; 1500 Illinois St. ; Golden ; CO ; 80401 ; USA
  4. Minnesota Department of Health ; Saint Paul ; MN ; 55164-0975 ; USA
  5. US Environmental Protection Agency ; 960 College Station Rd ; Athens ; GA ; 30605 ; USA
  6. Wageningen IMARES ; Haringkade 1 ; 1970 ; Ijmuiden ; The Netherlands
  7. Environmental Laboratory ; 3M Company ; 935 Bush Avenue ; St. Paul ; MN ; 55144 ; USA
  8. Water Science and Technology Directorate ; Environment Canada ; Burlington ; ON ; Canada
  9. US Environmental Protection Agency ; Research Triangle Park ; NC ; USA
  
• 关键词：Polyfluorinated substances ; Standard reference materials ; Sediment ; Sludge ; House dust ; Interlaboratory comparison exercise
• 刊名：Analytical and Bioanalytical Chemistry
• 出版年：2015
• 出版时间：April 2015
• 年：2015
• 卷：407
• 期：11
• 页码：2975-2983
• 全文大小：262 KB
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• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Analytical Chemistry
  Food Science
  Inorganic Chemistry
  Physical Chemistry
  Monitoring, Environmental Analysis and Environmental Ecotoxicology
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1618-2650

文摘

The National Institute of Standards and Technology (NIST) has a wide range of Standard Reference Materials (SRMs) which have values assigned for legacy organic pollutants and toxic elements. Existing SRMs serve as homogenous materials that can be used for method development, method validation, and measurement for contaminants that are now of concern. NIST and multiple groups have been measuring the mass fraction of a group of emerging contaminants, polyfluorinated substances (PFASs), in a variety of SRMs. Here we report levels determined in an interlaboratory comparison of up to 23 PFASs determined in five SRMs: sediment (SRMs 1941b and 1944), house dust (SRM 2585), soil (SRM 2586), and sludge (SRM 2781). Measurements presented show an array of PFASs, with perfluorooctane sulfonate being the most frequently detected. SRMs 1941b, 1944, and 2586 had relatively low concentrations of most PFASs measured while 23 PFASs were at detectable levels in SRM 2585 and most of the PFASs measured were at detectable levels in SRM 2781. The measurements made in this study were used to add values to the Certificates of Analysis for SRMs 2585 and 2781.