Mixed bismuth(III) complexes with sulfur donor ligands
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- 作者：H. P. S. Chauhan ; Sapana Joshi…
- 关键词：Dithiolates ; Bismuth(III) ; Thermal analyses ; EDAX ; Nanoparticles ; Powder XRD
- 刊名：Journal of Thermal Analysis and Calorimetry
- 出版年：2016
- 出版时间：April 2016
- 年：2016
- 卷：124
- 期：1
- 页码：117-130
- 全文大小：1,075 KB
- 参考文献：1.Cotton FA, Wilkinson G, Murillo CA, Bochmann M. Advanced inorganic chemistry. 6th ed. New York: Wiley; 1999.
2.Levason W, Reid G. Arsenic, antimony, and bismuth. In: Parkin GFR, editor. Comprehensive coordination chemistry II, vol. 3. Amsterdam: Elsevier; 2003. p. 465–544 [Chapter 3.6].CrossRef
3.Li M, Lu Y, Yang M, Li Y, Zhang L, Xie S. One dodecahedral bismuth(III) complex derived from 2-acetylpyridine N(4)-pyridylthiosemicarbazone: synthesis, crystal structure and biological evaluation. Dalton Trans. 2012;41:12882–7.CrossRef
4.Yang N, Sun HZ. Biocoordination chemistry of bismuth: recent advances. Coord Chem Rev. 2007;251:2354–66.CrossRef
5.Andrews PC, Ferrero RL, Junk PC, Kumar I, Luu Q, Nguyen K, Taylor JW. Bismuth(III) complexes derived from non-steroidal anti-inflammatory drugs and their activity against Helicobacter pylori. Dalton Trans. 2010;39:2861–8.CrossRef
6.Briand GG, Burford N. Bismuth compounds and preparations with biological or medicinal relevance. Chem Rev. 1999;99:2601–57.CrossRef
7.Beales ILP. Efficacy of Helicobacter pylori eradication therapies: a single centre observational study. BMC Gastroenterol. 2001;1:7–16.CrossRef
8.Leonard NM, Wieland LC, Mohan RS. Applications of bismuth(III) compounds in organic synthesis. Tetrahedron. 2002;58:8373–97.CrossRef
9.Carter RH. Insecticidal and fungicidal compositions. US patent 2150759; 1939.
10.Thorn GD, Ludwig RA. The dithiocarbamates and related compounds. New York: Elsevier Publication; 1962.
11.Cao SL, Feng YP, Jiang YY, Liu SY, Ding GY, Li RT. Synthesis and in vitro antitumor activity of 4(3H)-quinazolinone derivatives with dithiocarbamate side chains. Bioorg Med Chem Lett. 2005;15:1915–7.CrossRef
12.Buac D, Schmitt S, Ventro G, Kona FR, Ping Dou Q. Dithiocarbamate-based coordination compounds as potent proteasome inhibitors in human cancer cells. Mini Rev Med Chem. 2012;12:1193–201.CrossRef
13.Milacic V, Chen D, Ronconi L, Landis-Piwowar KR, Fregona D, Dou QP. A novel anticancer gold(III) dithiocarbamate compound inhibits the activity of a purified 20S proteasome and 26S proteasome in human breast cancer cell cultures and xenografts. Cancer Res. 2006;66:10478–86.CrossRef
14.Müller-Decker K. Interruption of TPA-induced signals by an antiviral and antitumoral xanthate compound: inhibition of a phospholipase c-type reaction. Biochem Biophys Res Commun. 1989;162:198–205.CrossRef
15.Amtmann E, Sauer G. Selective killing of tumor cells by xanthates. Cancer Lett. 1987;35:237–44.CrossRef
16.Burrage RH, Menzies JA, Zirk E. Soil treatment with broadcast or band applications of organophosphorus or carbamate insecticides for prevention of wireworm damage to potatoes. J Ecol Entomol. 1967;60:1489–92.CrossRef
17.Cohen SA, Antonis KMD. Applications of amino acid derivatization with 6-aminoquinolyl-N-hydroxysuccinimidyl carbamate: analysis of feed grains, intravenous solutions and glycoproteins. J Chromatogr A. 1994;661:25–34.CrossRef
18.Kočovský P. Carbamates: a method of synthesis and some synthetic applications. Tetrahedron Lett. 1986;27:5521–4.CrossRef
19.Gaur J, Jain S, Bhatia R, Lal A, Kaushik NK. Synthesis and characterization of a novel copolymer of glyoxal dihydrazone and glyoxal dihydrazone bis(dithiocarbamate) and application in heavy metal ion removal from water. J Therm Anal Calorim. 2013;112:1137–43.CrossRef
20.Buchanan RA, Weislogel E, Russell CR, Rist CE. Starch in rubber: zinc starch xanthate in latex masterbatching. Ind Eng Chem Prod Res Dev. 1968;7:155–8.CrossRef
21.Chen K, Grant N, Liang L, Zhang H, Tan B. Synthesis of CO2-philic xanthate-oligo(vinyl acetate)-based hydrocarbon surfactants by RAFT polymerization and their applications on preparation of emulsion-templated materials. Macromolecules. 2010;43:9355–64.CrossRef
22.Dias SC, Brasilino MGA, Pinheiro CD, Souza AG. Metal–sulphur bond enthalpy determination of diethyldithiocarbamate complexes of cadmium and mercury. Thermochim Acta. 1994;241:25–32.CrossRef
23.Carvalho MAP, Airoldi C, Souza AG. Thermochemical features of di-N-propyldithiocabamate chelates of zinc-group elements. J Chem Soc Dalton Trans. 1992;. doi:10.1039/DT9920001235 .
24.Carpenter J, Joshi S, Chauhan HPS. Ethane-1,2-dithiolato bridged (μ2) complexes of bis(N,N-diorganodithiocarbamato-S,S′)antimony(III). J Therm Anal Calorim. 2015;120:1203–15.CrossRef
25.Kropidłowska AM, Chojnacki J, Strankowski M, Fahmi A, Gazda M, Becker B. Cadmium complex possessing simultaneously silanethiolato and dithiocarbamato-ligands. A novel single-source precursor of cadmium sulfide. J Therm Anal Calorim. 2014;118:993–1001.CrossRef
26.Zhang Z, Cui ZL. Nanotechnology and nanomaterial. Beijing: National Defence Industry Publication; 2000.
27.Lu Q, Gao F, Komarneni S. Biomolecule-assisted synthesis of highly ordered snow flake like structures of bismuth sulfide nanorods. J Am Chem Soc. 2004;126:54–5.CrossRef
28.Liu L, Wang L, Yin H, Li Y, He X. The preparation and application of bismuth(III) ion-selective electrode based on nanoparticles of bismuth sulfide. Anal Lett. 2006;39:879–90.CrossRef
29.Chauhan HPS, Shaik NM, Singh UP. Synthesis, spectroscopic characterization and in vitro studies of antimicrobial activity of bis(diorganodithiocarbamato) organodithiocarbonatobismuth(III) complexes. Appl Organomet Chem. 2006;20:142–8.CrossRef
30.Chauhan HPS, Joshi S, Bakshi A, Carpenter J. Structural investigation on toluene-3,4-dithiolatoantimony(III) alkyldithiocarbonate complexes: thermal, powder XRD and biological studies. New J Chem. 2015;39:2279–88.CrossRef
31.Chauhan HPS, Bakshi A, Bhatiya S. Synthesis, spectroscopic characterization and antibacterial activity of antimony(III) bis(dialkyldithiocarbamato)alkyldithiocarbonates. Spectrochim Acta A. 2011;81:417–23.CrossRef
32.Koh YW, Lai CS, Du AY, Tiekink ERT, Loh KP. Growth of bismuth sulfide nanowire using bismuth trisxanthate single source precursors. Chem Mater. 2003;15:4544–54.CrossRef
33.Riddick JA, Bunger WB. Techniques of chemistry (organic solvents), vol. 2. New York: Wiley Interscience; 1970.
34.Magaldi S, Mata-Essayag S, De Capriles CH, Perez C, Colella MT, Olaizola C, Ontiveros Y. Well diffusion for antifungal susceptibility testing. Int J Infect Dis. 2004;8:39–45.CrossRef
35.Boyanova L, Gergova G, Nikolov R, Derejian S, Lazarova E, Katsarov N, Mitov I, Krastev Z. Activity of Bulgarian propolis against 94 helicobacter pylori strains in vitro by agar-well diffusion, agar dilution and disc diffusion methods. J Med Microbiol. 2005;54:481–3.CrossRef
36.Xiao G, Dong Q, Wang Y, Sui Y, Ning J, Liu Z, Tian W, Liu B, Zoua G, Zou B. One-step solution synthesis of bismuth sulfide (Bi2S3) with various hierarchical architectures and their photoresponse properties. RSC Adv. 2012;2:234–40.CrossRef
37.Chauhan HPS, Joshi S, Carpenter J. Synthetic, spectral, thermal and powder X-ray diffraction studies of bis(O-alkyldithiocarbonato-S,S′) antimony(III) dialkyldithiocarbamates. Spectrochim Acta A. 2015;136:1626–34.CrossRef
38.Manoussakis GE, Tsipis CA. Preparation and study of some arsenic and antimony tris dithiocarbamates. J Inorg Nucl Chem. 1973;35:743–50.CrossRef
39.Chauhan HPS, Bakshi A. Synthetic, spectroscopic, thermal, and structural studies of antimony(III) bis(pyrrolidinedithiocarbamato)alkyldithiocarbonates. J Therm Anal Calorim. 2011;105:937–46.CrossRef
40.Chauhan HPS, Carpenter J, Joshi S. Mixed bis(morpholine-4-dithiocarbamato-S, S′) antimony(III) complexes: synthesis, characterization and biological studies. Appl Organomet Chem. 2014;28:605–13.CrossRef
41.Chauhan HPS, Singh RK. Synthesis and characterization of bismuth(III) bis(dialkyldithiophosphate) alkyldithiocarbonate. Synth React Inorg Met-Org Chem. 2000;30(7):1211–9.CrossRef
42.Chauhan HPS, Shaik NM, Singh UP. Synthetic, spectroscopic and antimicrobial studies of bis(dialkyldithiocarbamato)diorganodithiophosphatobismuth(III) complexes. Appl Organomet Chem. 2005;19:1132–9.CrossRef
43.Bailey JHE, Drake JE, Khasrou LN, Yang J. Synthesis and spectroscopic characterization of O-alkyl dithiocarbonate (xanthate) derivatives of dimethyl- and diphenyltellurium(IV) crystal structures of Me2Te[S2COEt]2 and Ph2Te[S2COEt]2. Inorg Chem. 1995;34:124–33.CrossRef
44.Van Gaal HLM, Diesveld JW, Pijpers FW, Van Der Linden JGM. 13C NMR spectra of dithiocarbamates chemical shifts, carbon–nitrogen stretching vibration frequencies, and p bonding in the NCS2 fragment. Inorg Chem. 1979;18:3251–60.CrossRef
45.Cullity BD. Elements of X-ray diffraction. Reading: Addison-Wesley Publishing Company; 1958.
46.Klug HP, Alexander LE. X-ray diffraction procedures for polycrystalline and amorphous materials. New York: Wiley; 1974. - 作者单位：H. P. S. Chauhan (1)
Sapana Joshi (1)
Jaswant Carpenter (1)
1. School of Chemical Sciences, Devi Ahilya University (NAAC ‘A’ Grade), Takshashila Campus, Khandwa Road, Indore, 452001, India - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Sciences
Polymer Sciences
Physical Chemistry
Inorganic Chemistry
Measurement Science and Instrumentation - 出版者：Akad茅miai Kiad贸, co-published with Springer Science+Business Media B.V., Formerly Kluwer Academic
- ISSN：1572-8943
文摘
Mixed bismuth(III) bis(O-alkyldithiocarbonato-S,S′) complexes with dialkyldithiocarbamates have been obtained by two-step one-pot synthesis. These complexes have been characterized by physicochemical (molecular mass determination, melting point and elemental analysis), spectral (UV–Visible, FTIR, far-IR, 1H and 13C NMR), thermal and powder X-ray diffraction studies. It has been observed that both the dithiolato ligands are coordinated via an anisobidentate mode to the central metal atom. Powder XRD analysis indicates that all the complexes are in nanoranged crystallite size (3.1–8.8 nm) and have adopted monoclinic crystal system. Bismuth sulfide (Bi2S3) nanoparticles have been obtained upon thermal decomposition of these complexes. The preparation of bismuth sulfide (Bi2S3) nanoparticles was further confirmed by the help of EDAX analysis of the thermal degradation product. All the synthesized complexes exhibited greater antimicrobial activity than standard antibacterial drug chloramphenicol and antifungal drug terbinafine.