Non-isothermal crystallization kinetics of sucrose palmitate reinforced poly(lactic acid) bionanocomposites

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• 作者：Ravibabu Valapa ; Sameer Hussain ; Parmeswar Krishnan Iyer…
• 关键词：Sucrose palmitate ; Poly(lactic acid) ; Differential scanning calorimetry ; Non ; isothermal crystallization kinetics ; Avrami model ; Polarized optical microscopy
• 刊名：Polymer Bulletin
• 出版年：2016
• 出版时间：January 2016
• 年：2016
• 卷：73
• 期：1
• 页码：21-38
• 全文大小：3,905 KB
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• 作者单位：Ravibabu Valapa (1)
  Sameer Hussain (2)
  Parmeswar Krishnan Iyer (2)
  G. Pugazhenthi (1)
  Vimal Katiyar (1)
  
  1. Department of Chemical Engineering, Indian Institute of Technology Guwahati, Guwahati, 781039, Assam, India
  2. Department of Chemistry, Indian Institute of Technology Guwahati, Guwahati, 781039, Assam, India
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Polymer Sciences
  Characterization and Evaluation Materials
  Soft Matter and Complex Fluids
  Physical Chemistry
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1436-2449

文摘

Poly(lactic acid) (PLA) bionanocomposites containing sucrose palmitate (SP), which is a non-toxic food additive, were prepared by a simple solution-casting approach. In the current work, the investigation of non-isothermal cold crystallization kinetics of PLA and PLA–SP bionanocomposites was performed using a differential scanning calorimeter under the dynamic heating regime of 2.5, 5, 7.5 and 10 °C/min. Avrami model was employed to study the effect of SP on cold crystallization kinetics of PLA. For PLA–SP bionanocomposites, Avrami coefficients obtained in the range of ~2.5–4 and decreasing trend of the t _1/2 values indicated the faster crystallization mechanism in comparison to neat PLA. The nucleation and growth mechanism involved in the non-isothermal crystallization of PLA and PLA–SP bionanocomposites were further analyzed by Tobin model. Kissinger method has been employed to determine the crystallization activation energy (ΔE) for neat PLA and PLA–SP bionanocomposite. The nucleation as well as the growth of spherulites in neat PLA and PLA–SP bionanocomposites was observed using polarized optical microscopy. After incorporation of SP in the PLA matrix, an increase in the overall crystallization rate for PLA was reflected by the decline in the nucleation induction period and subsequent enhancement in the primary nucleation sites.