Determination of Octenylsuccinic Acid in Nutritional Products

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• 作者：Paul W. Johns ; Wesley A. Jacobs ; Maggie M. Hroncich…
• 关键词：Octenylsuccinic acid ; Nutritional product ; Modified starch ; Emulsifier ; LC/UV
• 刊名：Food Analytical Methods
• 出版年：2015
• 出版时间：March 2015
• 年：2015
• 卷：8
• 期：3
• 页码：807-814
• 全文大小：307 KB
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• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Food Science
  Chemistry
  Microbiology
  Analytical Chemistry
  
• 出版者：Springer New York
• ISSN：1936-976X

文摘

A quantitative method for the direct LC/UV determination of octenylsuccinic acid (OSAc) in nutritional products formulated with octenylsuccinic anhydride-modified starch (MS) is described. The cis-2-OSAc and trans-2-OSAc released from the MS by a mild alkaline hydrolysis are separated by reversed phase chromatography and are detected by UV at 192?nm. Method suitability has been defined by assessments of linearity (R 2 average--.99991?±-.00008, n--2, and the relative calibration error average