Determination of cadmium(II) using carbon paste electrode modified with a Cd-ion imprinted polymer

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• 作者：Hamid Ashkenani (12) hamid6730@gmail.com
  Mohammad Ali Taher (1)
• 关键词：Cd(II) – Ion ; imprinted polymer – Modified carbon paste electrode – Voltammetry – Water and food samples
• 刊名：Microchimica Acta
• 出版年：2012
• 出版时间：July 2012
• 年：2012
• 卷：178
• 期：1-2
• 页码：53-60
• 全文大小：333.4 KB
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• 作者单位：1. Department of Chemistry, Shahid Bahonar University of Kerman, Kerman, Iran2. Young Researchers Society, Shahid Bahonar University of Kerman, P.O. Box 76175-133, Kerman, Iran
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Analytical Chemistry
  Inorganic Chemistry
  Physical Chemistry
  Characterization and Evaluation Materials
  Monitoring, Environmental Analysis and Environmental Ecotoxicology
  
• 出版者：Springer Wien
• ISSN：1436-5073

文摘

We have synthesized cadmium(II) ion-imprinted polymers (IIP) and non-imprinted polymers (NIP) using 1-(2-pyridylazo)-2-naphthol as a ligand. The materials were used to prepare a carbon paste electrode for the determination of Cd(II). Polymerization was performed with (a) methacrylic acid as a functional monomer, (b) ethyleneglycol dimethacrylate as the crosslinking monomer, and (c) 2,2′-azobis(isobutyronitrile) as the initiator. Imprinted cadmium ion was removed from the polymeric matrix using nitric acid. The measurements were carried out in an closed circuit after accumulation at ?1.2 V, this followed by electrolysis of the accumulated Cd(II) by voltammetric scanning from ?1.0 to ?0.6 V. The parameters governing the response of the electrode were studied. Under optimized conditions, the response of the electrode is linear in the range from 2.0 to 200 ng mL?1. The detection limit is 0.31 ng mL?1. The relative standard deviations are ±3.4 and ±2.1 % for 7 successive determinations of 20.0 and 50.0 ng mL-1 of Cd(II), respectively. The method was applied to the determination of cadmium (II) in water and food samples.