Electrochemical synthesis of Fe/Al-layered double hydroxide on a glassy carbon electrode: application for electrocatalytic reduction of isoniazid

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• 作者：Karim Asadpour-Zeynali ; Yasin Shabangoli…
• 关键词：Layered double hydroxide (LDH) ; Differential pulse voltammetry ; Isoniazid (INZ) ; Glassy carbon electrode (GCE) ; Determination
• 刊名：Journal of the Iranian Chemical Society
• 出版年：2016
• 出版时间：January 2016
• 年：2016
• 卷：13
• 期：1
• 页码：29-36
• 全文大小：1,417 KB
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• 作者单位：Karim Asadpour-Zeynali (1)
  Yasin Shabangoli (1)
  Kamellia Nejati (2)
  
  1. Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, Iran
  2. Chemistry Department, Payame Noor University, PO. Box 19395-3697, Tehran, Iran
  
• 刊物主题：Analytical Chemistry; Inorganic Chemistry; Physical Chemistry; Biochemistry, general; Organic Chemistry;
• 出版者：Springer Berlin Heidelberg
• ISSN：1735-2428

文摘

Fe/Al-layered double hydroxide (Fe/Al-LDH) was synthesized on a glassy carbon electrode (GCE) by a novel and simple electrochemical method. The electrochemical characterization of Fe/Al-LDH deposited on GCE was investigated in a 0.1 M NaOH solution. Moreover, the LDH film obtained was characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, scanning electron microscopy (SEM), and energy dispersive X-ray (EDX). The obtained results showed that Fe/Al-LDH was generated on GCE by the electrochemical method, and that the obtained film was highly pure. The electrochemical behavior of isonicotinic acid hydrazide or isoniazid (INZ) at LDH/GCE was studied by the electrochemical techniques including cyclic voltammetry, differential pulse voltammetry, and amperometry. The obtained results indicated an excellent electrocatalytic reduction activity for the Fe/Al-LDH-modified GCE of INZ. Under the optimized conditions for determination of INZ the calibration curves are linear in the ranges of 4.9–650.0 and 4.9–770.0 μM with limit of detections of 4.0 and 7.0 μM for differential pulse voltammetry, and amperometry techniques, respectively. The proposed method was performed successfully the analysis of INZ in commercial drugs.