The influence of Si as reactive bonding agent in the electrophoretic coatings of HA–Si–MWCNTs on NiTi alloys
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- 作者：Vida Khalili ; Jafar Khalil-Allafi…
- 关键词：carbon nanotubes ; electrophoretic deposition ; hydroxyapatite ; reactive bonding ; silicon ; sintering
- 刊名：Journal of Materials Engineering and Performance
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：25
- 期：2
- 页码：390-400
- 全文大小：5,906 KB
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Jafar Khalil-Allafi (1)
Hossein Maleki-Ghaleh (1)
Alexander Paulsen (3)
Jan Frenzel (3)
Gunther Eggeler (3)
1. Research Center for Advanced Materials and Mineral Processing, Faculty of Materials Engineering, Sahand University of Technology, Tabriz, Iran
2. Department of Mechanical Engineering, University of Bonab, Velayat Highway, P.O.Box: 5551761167, Bonab, Iran
3. Institute for Materials Science, Faculty of Mechanical Engineering, Ruhr-University Bochum, 44801, Bochum, Germany - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Characterization and Evaluation Materials
Materials Science
Tribology, Corrosion and Coatings
Quality Control, Reliability, Safety and Risk
Engineering Design - 出版者：Springer New York
- ISSN：1544-1024
文摘
In this study, different composite coatings with 20 wt.% silicon and 1 wt.% multi-walled carbon nanotubes of hydroxyapatite were developed on NiTi substrate using a combination of electrophoretic deposition and reactive bonding during the sintering. Silicon was used as reactive bonding agent. During electrophoretic deposition, the constant voltage of 30 V was applied for 60 s. After deposition, samples were dried and then sintered at 850 °C for 1 h in a vacuum furnace. SEM, XRD and EDX were used to characterize the microstructure, phase and elemental identification of coatings, respectively. The SEM images of the coatings reveal a uniform and compact structure for HA–Si and HA–Si–MWCNTs. The presence of silicon as a reactive bonding agent as well as formation of new phases such as SiO2, CaSiO3 and Ca3SiO5 during the sintering process results in compact coatings and consumes produced phases from HA decomposition. Formation of the mentioned phases was confirmed using XRD analysis. The EDX elemental maps show a homogeneous distribution of silicon all over the composite coatings. Also, the bonding strength of HA–Si–MWCNTs coating is found to be 27.47 ± 1 MPa. Keywords carbon nanotubes electrophoretic deposition hydroxyapatite reactive bonding silicon sintering