Determination of organogenic elements in the composition of functional compounds and materials

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• 作者：V. P. Fadeeva (1)
  V. D. Tikhova (1)
  Yu. M. Deryabina (1)
  O. N. Nikulicheva (1)
  
• 关键词：elemental analysis ; organogenic elements ; oxide catalytic compositions ; functional compounds and materials
• 刊名：Journal of Structural Chemistry
• 出版年：2014
• 出版时间：September 2014
• 年：2014
• 卷：55
• 期：5
• 页码：972-979
• 全文大小：201 KB
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• 作者单位：V. P. Fadeeva (1)
  V. D. Tikhova (1)
  Yu. M. Deryabina (1)
  O. N. Nikulicheva (1)
  
  1. Vorozhtsov Institute of Organic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia
  
• ISSN：1573-8779

文摘

The presented analysis methods (automatic and gravimetric) are used to determine the main composition of various organic functional materials such as paramagnetic chelating agents for the synthesis of molecular magnetics, polyfluoroaromatic compounds for the preparation of special latices, new antivirus and analgesic agents, photoinitiator compounds for cationic polymerization, fluorophores for organic light emitting diodes, and so on. Conditions for the quantitative formation of final products of the complete decomposition of the compound (CO2, H2O, N2, SO2) are shown: the application of special oxide catalytic compositions and also the use of selectively adsorbing reagents for the removal of compounds hindering the determination of organogenic elements. Their determination error does not exceed ±0.3 % abs.