Fabrication and properties of cellulose-nanochitosan biocomposite film using ionic liquid

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• 作者：Farzam Niroomand ; Amir Khosravani ; Habibollah Younesi
• 关键词：Nanochitosan ; Nano ; biocomposite ; Cellulose film ; Cellulose dissolution ; Ionic liquid
• 刊名：Cellulose
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：23
• 期：2
• 页码：1311-1324
• 全文大小：2,276 KB
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• 作者单位：Farzam Niroomand (1)
  Amir Khosravani (1)
  Habibollah Younesi (2)
  
  1. Department of Wood and Paper Science and Technology, Faculty of Natural Resources, Tarbiat Modares University, Noor, Iran
  2. Department of Environmental Science, Faculty of Natural Resources, Tarbiat Modares University, Noor, Iran
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Bioorganic Chemistry
  Physical Chemistry
  Organic Chemistry
  Polymer Sciences
  
• 出版者：Springer Netherlands
• ISSN：1572-882X

文摘

Chitosan is a widely used biopolymer with very attractive properties. However, to compensate for the deficiencies in the application of this bio-macromolecule, many studies have been performed on the preparation of chitosan blends with various polymers, such as cellulose, which is abundant and unique with a tough bio-structure. Because of the different dissolution conditions of chitosan and cellulose, an acceptable industrial and environmentally friendly process to prepare a monotonous cellulose-chitosan composite film has not been achieved yet. Therefore, as an alternative approach, nanochitosan (Nano-CS) particles were synthesized and blended with a cellulose matrix, which was dissolved using ionic liquid. Atomic force microscope and field emission scanning electron microscope (FESEM) images demonstrated that the most frequent size of Nano-CS particles was in the 10–60 nm range. FESEM nano-graphs evidenced monotonous distribution of Nano-CS particles through the produced nano-biocomposite films. X-ray diffractograms indicated that following the dissolution process of cellulose a less ordered cellulose matrix or one with less crystallite sizes was formed. Meanwhile, following the addition of certain amounts of Nano-CS, the mechanical properties were improved. Also, optical analysis exhibited proper transparency of the biocomposite films (≈80 %) in the range of visible wavelengths (400–700 nm).