Interaction between chiral ions: synthesis and characterization of tartratovanadates(V) with tris(2,2-bipyridine) complexes of iron(II) and nickel(II) as cations
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- 作者：Peter Antal ; Peter Schwendt ; Jozef Tatiersky ; Róbert Gyepes…
- 刊名：Transition Metal Chemistry
- 出版年：2014
- 出版时间：November 2014
- 年：2014
- 卷：39
- 期：8
- 页码：893-900
- 全文大小：979 KB
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Peter Schwendt (1)
Jozef Tatiersky (1)
Róbert Gyepes (2) (3)
Milan Drábik (1) (4)
1. Department of Inorganic Chemistry, Faculty of Natural Sciences, Comenius University, Mlynská dolina, 842 15, Bratislava, Slovak Republic
2. Faculty of Education, J. Selye University, Bratislavská cesta 3322, 945 01, Komárno, Slovak Republic
3. J. Heyrovsky Institute of Physical Chemistry of the AS CR, v.v.i., Dolej?kova 3, 182 23, Prague 8, Czech Republic
4. Institute of Inorganic Chemistry, Slovak Academy of Sciences, Dúbravská cesta 9, 845 36, Bratislava 45, Slovak Republic - ISSN：1572-901X
文摘
Four new compounds composed of chiral complex cations and anions: Δ-[Fe(bpy)3] Λ-[Fe(bpy)3][V4O8((2R,3R)-tart)2]·12H2O (1), Δ-[Fe(bpy)3]2Λ-[Fe(bpy)3]2[V4O8((2R,3R)-tart)2][V4O8((2S,3S)-tart)2]·24H2O (2), Δ-[Ni(bpy)3]Λ-[Ni(bpy)3][V4O8((2R,3R)-tart)2]·12H2O (3) and Δ-[Ni(bpy)3]2Λ-[Ni(bpy)3]2[V4O8((2R,3R)-tart)2][V4O8((2S,3S)-tart)2]·24H2O (4) have been prepared. The compounds have been characterized by spectral methods, and their thermal decomposition was studied by simultaneous DTA, TG measurements. The final products after dynamic decomposition and additional heating were Fe2V4O13 for 1 and 2 and Ni(VO3)2 for 3 and 4. The crystal structures determined for 1, 2 and 4 have evidenced that 1 is “hemiracemic-and 2 and 4 are “fully racemic-compounds.