A highly sensitive nonenzymatic glucose sensor based on nickel oxide–carbon nanotube hybrid nanobelts

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• 作者：Wei Yi (1)
  Duanguang Yang (1)
  Hongbiao Chen (1)
  Pengcheng Liu (1)
  Jian Tan (1)
  Huaming Li (1) (2) (3) (4)
  
• 关键词：Glucose ; Single ; walled carbon nanotubes ; NiO nanobelts ; Electrooxidation ; Nonenzymatic sensor
• 刊名：Journal of Solid State Electrochemistry
• 出版年：2014
• 出版时间：April 2014
• 年：2014
• 卷：18
• 期：4
• 页码：899-908
• 全文大小：1,260 KB
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• 作者单位：Wei Yi (1)
  Duanguang Yang (1)
  Hongbiao Chen (1)
  Pengcheng Liu (1)
  Jian Tan (1)
  Huaming Li (1) (2) (3) (4)
  
  1. College of Chemistry, Xiangtan University, Xiangtan, 411105, Hunan Province, China
  2. Key Laboratory of Polymeric Materials and Application Technology of Hunan Province, Xiangtan University, Xiangtan, 411105, Hunan Province, China
  3. Key Laboratory of Advanced Functional Polymeric Materials of College of Hunan Province, Xiangtan University, Xiangtan, 411105, Hunan Province, China
  4. Key Laboratory of Environment-Friendly Chemistry and Application in Ministry of Education, Xiangtan University, Xiangtan, 411105, Hunan Province, China
  
• ISSN：1433-0768

文摘

In this study, we demonstrated a highly sensitive electrochemical sensor for the determination of glucose in alkaline aqueous solution by using nickel oxide single-walled carbon nanotube hybrid nanobelts (NiO–SWCNTs) modified glassy carbon electrode (GCE). The hybrid nanobelts were prepared by the deposition of SWCNTs onto the Ni(SO4)0.3(OH)1.4 nanobelt surface, followed by heat treatment at different temperatures ranging from 400?°C to 600?°C. The NiO–SWCNTs hybrid nanobelts modified electrode prepared at 500?°C displays enhanced electrocatalytic activity towards glucose oxidation, revealing a synergistic effect between the NiO and the deposited SWCNTs. The as-fabricated nonenzymatic glucose sensor exhibits excellent glucose sensitivity (2,980?μA?cm??mM?), lower detection limit (0.056?μM, signal/noise [S/N] ratio--), and wider linear range (0.5-,300?μM). Moreover, the sensor has been successfully used for the assay of glucose in serum samples with good recovery, ranging from 96.4?% to 102.4?%.