Hydrothermal syntheses and photocatalytic performance of three Mn-based coordination complexes constructed from 1,10-phenanthroline and polycarboxylic acids

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• 作者：Chong-Chen Wang ; Fang Gao ; Xin-Xing Guo ; Huan-Ping Jing…
• 刊名：Transition Metal Chemistry
• 出版年：2016
• 出版时间：May 2016
• 年：2016
• 卷：41
• 期：4
• 页码：375-385
• 全文大小：1,942 KB
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• 作者单位：Chong-Chen Wang (1) (2)
  Fang Gao (1)
  Xin-Xing Guo (1)
  Huan-Ping Jing (1)
  Peng Wang (1)
  Shi-Jie Gao (1)
  
  1. Key Laboratory of Urban Stormwater System and Water Environment (Ministry of Education), Beijing, 100044, China
  2. Beijing Engineering Research Center of Sustainable Urban Sewage System Construction and Risk Control, Beijing University of Civil Engineering and Architecture, Beijing, 100044, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Physical Chemistry
  Inorganic Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1572-901X

文摘

Three coordination complexes based on manganese, namely Mn(phen)(5-Br-ipa) (1), Mn(phen)(5-NO₂-ipa) (2), and [Mn(phen)₂(3,4-H₂dczpb)]·H₂O (3) (phen = 1,10-phenanthroline; 5-Br-ipa = 5-bromoisophthalic acid; 5-NO₂-ipa = 5-nitroisophthalic acid; 3,4-H₄dczpb = 3,4-dicarboxyl-(3′,4′-dicarboxylazophenyl)benzene), have been synthesized under hydrothermal conditions and characterized by single-crystal X-ray diffraction, FTIR, elemental analysis, and UV–Vis diffuse reflection spectroscopy. The photocatalytic efficiencies of the complexes for the decomposition of methylene blue under UV irradiation were also investigated. These complexes show 2D sheet, 1D chain and 0D discrete structures due to the different coordination environments of the Mn(II) centers and the number of phen ligands.