Fabrication of a Substituted Imidazolate Material 1 (SIM-1) membrane using post synthetic modification (PSM) for pervaporation of water/ethanol mixtures

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• 作者：Anne M. Marti ; Daniel Tran ; Kenneth J. Balkus Jr.
• 关键词：Metal organic framework ; MOF ; Zeolitic imidazolate framework ; ZIF ; Substituted Imidazolate Material 1 ; SIM ; 1 ; SIM ; 1 membrane ; Linker exchange ; Pervaporation
• 刊名：Journal of Porous Materials
• 出版年：2015
• 出版时间：October 2015
• 年：2015
• 卷：22
• 期：5
• 页码：1275-1284
• 全文大小：2,270 KB
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• 作者单位：Anne M. Marti (1)
  Daniel Tran (1)
  Kenneth J. Balkus Jr. (1)
  
  1. Department of Chemistry, University of Texas at Dallas, 800 West Campbell Road, Richardson, TX, 75080, USA
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Characterization and Evaluation Materials
  Physical Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1573-4854

文摘

Post synthetic modification (PSM) of metal organic frameworks (MOFs) is a useful tactic used amongst researchers to refine a MOF’s properties for an application of interest. In this report, we post synthetically modified a MOF known as Substituted Imidazolate Material 1 (SIM-1) to refine its molecular sieving potential. PSM of ethylenediamine, EDA, vapor was applied to a SIM-1 wafer. EDA cross-linked MOF crystals together through a Schiff base condensation reaction with SIM-1’s reactive aldehyde linker forming a free- standing SIM-1 membrane. The membranes were tested for the separation of water from water/ethanol mixtures at room temperature. Results show that only water was detected by GC for all SIM-1 membrane permeates; this was consistent over the course of three separation cycles, whereas SIM-1 wafers without PSM fall apart after one separation cycle. Keywords Metal organic framework MOF Zeolitic imidazolate framework ZIF Substituted Imidazolate Material 1 SIM-1 SIM-1 membrane Linker exchange Pervaporation