Facile synthesis of nanocrystalline Fe/Fe3C induced by bromide

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• 作者：Jiajia Gao ; Xiaobai Wang ; Xin Pan…
• 刊名：Journal of Materials Science: Materials in Electronics
• 出版年：2016
• 出版时间：January 2016
• 年：2016
• 卷：27
• 期：1
• 页码：64-69
• 全文大小：678 KB
• 参考文献：1.S. Behrens, Nanoscale 3, 877–892 (2011)CrossRef
  2.S. Laurent, D. Forge, M. Port, A. Roch, C. Robic, L. Vander Elst, R.N. Muller, Chem. Rev. 108, 2064–2110 (2008)CrossRef
  3.Z. Schnepp, S.C. Wimbush, M. Antonietti, C. Giordano, Chem. Mater. 22, 5340–5344 (2010)CrossRef
  4.C. Yang, H. Zhao, Y. Hou, D. Ma, J. Am. Chem. Soc. 134, 15814–15821 (2012)CrossRef
  5.A.A. Kuznetsov, V.I. Filippov, O.A. Kuznetsov, V.G. Gerlivanov, E.K. Dobrinsky, S.I. Malashin, J. Magn. Magn. Mater. 194, 22–30 (1999)CrossRef
  6.S. Mornet, S. Vasseur, F. Grasset, E. Duguet, J. Mater. Chem. 14, 2161–2175 (2004)CrossRef
  7.X. Wang, P. Zhang, W. Wang, X. Lei, B. Zou, H. Yang, RSC Adv. 5, 27857–27861 (2015)CrossRef
  8.Y. Wang, B.H. Davis, Appl. Catal. A 180, 277–285 (1999)CrossRef
  9.C. Giordano, A. Kraupner, S.C. Wimbush, M. Antonietti, Small 6, 1859–1862 (2010)CrossRef
  10.E.P. Sajitha, V. Prasad, S.V. Subramanyam, M. Ajay Kumar, S. Subhajit, B. Chandrahaas, J. Phys.: Condens. Matter. 19, 046214 (2007)
  11.I.K. Herrmann, R.N. Grass, D. Mazunin, W.J. Stark, Chem. Mater. 21, 3275–3281 (2009)CrossRef
  12.V. Amendola, P. Riello, M. Meneghetti, J. Phys. Chem. C 115, 5140–5146 (2011)CrossRef
  13.C.P. Deck, K. Vecchio, Carbon 44, 267–275 (2006)CrossRef
  14.J.A. Nelson, M.J. Wagner, Chem. Mater. 14, 4460–4463 (2002)CrossRef
  15.U. Narkiewicz, N. Guskos, W. Arabczyk, J. Typek, T. Bodziony, W. Konicki, G. Gąsiorek, I. Kucharewicz, E.A. Anagnostakis, Carbon 42, 1127–1132 (2004)CrossRef
  16.D.W. Lee, J.H. Yu, B.K. Kim, T.S. Jang, J. Alloys Compd. 449, 60–64 (2008)CrossRef
  17.N. Fan, X. Ma, Z. Ju, J. Li, Mater. Res. Bull. 43, 1549–1554 (2008)CrossRef
  18.A. Wu, D. Liu, L. Tong, L. Yu, H. Yang, CrystEngComm 13, 876–882 (2011)CrossRef
  19.C. Schliehe, J. Yuan, S. Glatzel, K. Siemensmeyer, K. Kiefer, C. Giordano, Chem. Mater. 24, 2716–2721 (2012)CrossRef
  20.A. Meffre, B. Mehdaoui, V. Kelsen, P.F. Fazzini, J. Carrey, S. Lachaize, M. Respaud, B. Chaudret, Nano Lett. 12, 4722–4728 (2012)CrossRef
  21.Z. Schnepp, M. Thomas, S. Glatzel, K. Schlichte, R. Palkovits, C. Giordano, J. Mater. Chem. 21, 17760–17764 (2011)CrossRef
  22.A.M. Nartowski, I.P. Parkin, A.J. Craven, M. MacKenzie, Adv. Mater. 10, 805–808 (1998)CrossRef
  23.A.M. Nartowski, I.P. Parkin, M. Mackenzie, A.J. Craven, J. Mater. Chem. 11, 3116–3119 (2001)CrossRef
  24.J.B. Wiley, R.B. Kaner, Sci. 255, 1093–1097 (1992)CrossRef
  25.E.G. Gillan, R.B. Kaner, Chem. Mater. 8, 333–343 (1996)CrossRef
  26.B. Jürgens, E. Irran, J. Senker, P. Kroll, H. Müller, W. Schnick, J. Am. Chem. Soc. 125, 10288–10300 (2003)CrossRef
  27.V.N. Khabashesku, J.L. Zimmerman, J.L. Margrave, Chem. Mater. 12, 3264–3270 (2000)CrossRef
  28.E.G. Gillan, Chem. Mater. 12, 3906–3912 (2000)CrossRef
  29.B.V. Lotsch, W. Schnick, Chem. Mater. 17, 3976–3982 (2005)CrossRef
  30.H. Zhao, M. Lei, X.A. Yang, J. Jian, X. Chen, J. Am. Chem. Soc. 127, 15722–15723 (2005)CrossRef
  31.A. Tapase, R. Patil, S. Delekar, I. Mulla, P. Hankare, J. Mater. Sci.: Mater. Electron. 25, 369–375 (2014)
  32.X. Huang, B. Dai, Y. Ren, J. Xu, C. Zhao, J. Mater. Sci.: Mater. Electron. 26, 2584–2588 (2015)
  33.Y. Jin, H. Zhu, Y. Xu, Y. Jin, Z. Xu, J. Mater. Sci.: Mater. Electron. 26, 4325–4329 (2015)
  34.R. Xiang, S.X. Zhou, B.S. Dong, G.Q. Zhang, Z.Z. Li, Y.G. Wang, J. Mater. Sci.: Mater. Electron. 25, 2979–2984 (2014)
  
• 作者单位：Jiajia Gao (1)
  Xiaobai Wang (1)
  Xin Pan (2)
  Xiaozhen Ren (1)
  Yu Han (3)
  Xuwei Yang (1)
  Hua Yang (1)
  
  1. College of Chemistry, Jilin University, Changchun, 130012, China
  2. Department of Ophthalmology, The Second Hospital of Jilin University, Changchun, 130041, China
  3. Department of Chemistry, College of Science, Yanbian University, Yanji, 133002, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Optical and Electronic Materials
  Characterization and Evaluation Materials
  
• 出版者：Springer New York
• ISSN：1573-482X

文摘

Fe₃C is a promising material with both high saturation magnetization and chemical stability. In this article, we present a facile sol–gel route for the synthesis of Fe₃C/Fe nanocomposites, in which bromide was found to be the inducing agent for the conversion of FeCl₃ to Fe₃C. X-ray diffraction, transmission electron microscopy, and vibrating sample magnetometer were used to characterize the composites. The experimental results show that the composition and magnetic properties of Fe₃C/Fe composites can be controlled by changing reaction temperatures, reaction time and the amount of inducing agent. Moreover, the possible formation mechanism of as-prepared nanostructures is discussed.