Synthesis and crystal structure of p-tert-butylcalix[4]arene 1,3-distal and monosubstituted semicarbazones and thiosemicarbazones

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• 作者：Zhenming Liu (1)
  Dongmei Liu (2)
  Jinxiang Wang (2)
  Jing Sun (2)
  Chaoguo Yan (2)
  
• 关键词：Calixarene ; Semicarbazide ; Semicarbazone ; Thiosemicarbazone ; Schiff base ; Crystal structure
• 刊名：Chemical Research in Chinese Universities
• 出版年：2014
• 出版时间：June 2014
• 年：2014
• 卷：30
• 期：3
• 页码：415-419
• 全文大小：
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• 作者单位：Zhenming Liu (1)
  Dongmei Liu (2)
  Jinxiang Wang (2)
  Jing Sun (2)
  Chaoguo Yan (2)
  
  1. Analysis and Test Center, Yangzhou University, Yangzhou, 225002, P. R. China
  2. College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou, 225002, P. R. China
  
• ISSN：2210-3171

文摘

A series of p-tert-butylcalix[4]arene 1,3-distal and monosubstituted semicarbazones and thiosemicarbazones was preparedd by acid catalyzed condensation reaction of active calixarene aldehydes with semicarbazide and thiocarbazide in methanol. One representative single crystal was determined by X-ray dirraction method, which shows that calixarene exists in cone configuration and intramolecular hydrogen-bands exist in the crystal.