Cobalt(II) and silver(I) coordination polymers constructed from flexible bis(5,6-dimethylbenzimidazole) and substituted isophthalate co-ligands

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• 作者：Rui Yang (1)
  Kristof Van Hecke (2)
  Bao Yi Yu (2)
  Guang Yue Li (1)
  Guang Hua Cui (1)
  
• 刊名：Transition Metal Chemistry
• 出版年：2014
• 出版时间：August 2014
• 年：2014
• 卷：39
• 期：5
• 页码：535-541
• 全文大小：996 KB
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• 作者单位：Rui Yang (1)
  Kristof Van Hecke (2)
  Bao Yi Yu (2)
  Guang Yue Li (1)
  Guang Hua Cui (1)
  
  1. College of Chemical Engineering, Hebei United University, 46 West Xinhua Road, Tangshan, 063009, Hebei, People’s Republic of China
  2. Department of Inorganic and Physical Chemistry, Ghent University, Krijgslaan 281 S3, 9000, Ghent, Belgium
  
• ISSN：1572-901X

文摘

Two coordination polymers, [Co(L1)(IPA] n (1) and {[Ag(L2)(HMIPA)]·H2O} n (2) (H2IPA?=?isophthalic acid, L1?=?1,2-bis(5,6-dimethylbenzimidazol-1-ylmethyl)benzene, H2MIPA?=?5-methylisophthalic acid, L2?=?1,6-bis(5,6-dimethylbenzimidazol-1-yl)hexane, have been synthesized and characterized by physicochemical and spectroscopic methods, as well as single-crystal X-ray diffraction. In 1, six-coordinated cobalt centers are bridged by L1 and IPA2?/sup> ligands to generate a (4,4) two-dimensional layer. However, complex 2 features a 1D chain structure, which is further extended by O–H···O hydrogen bonding interactions into a 2D supramolecular layer with (63) topology. The fluorescence and thermal gravimetric analysis of both complexes were also explored. Furthermore, the complexes 1 and 2 exhibit remarkable catalytic properties for the degradation of methyl orange dyes in a Fenton-like process.